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International Textile Manufacturers Federation (ITMF)

International Cotton CommitteeInternational Cotton Committee on Testing Methods (ICCTM)

Stickiness WG

Introduction

GOURLOT Jean-Paul Bremen March 2010

CIRAD UPR102

Bremen, March 2010

Laboratoire de Technologie et de Caractérisationdes fibres naturelles

Agenda of the ITMF meetingStickiness WG/TFStickiness WG/TF

Gourlot J.-P., CIRADIntroduction bibliography and latest informationIntroduction, bibliography and latest information

Gozé E., CIRADMeasurements based on counts : variability and methods of analysis

Harzallah O., ENSISA LPMTAdhesion Energy study of some Physiological and d es o e gy s udy o so e ys o og ca a dEntomological sugars

Plan of presentation

I t d tiIntroduction

Stickiness: origins

Stickiness: measurementStickiness: measurement

Introduction

The challenge for cotton today

To remaincompetitive with

To maintainacceptable profitability incompetitive with

synthetic fibersacceptable profitability in

production

Reduction of the production and processing costs

Introduction

The challenge for cotton today

Cotton fiber stickiness Defects / Disruptions ofCotton fiber stickiness Defects / Disruptions of the spinning processes

Classer

Trader

SpinnerResearcher

Producer

p

P i di tHigher spinning costLower yarn quality

Price discount

Additional operationsLower yarn quality

Plan of presentation

I t d tiIntroduction

Stickiness: origins

Stickiness: measurementStickiness: measurement

Origins of stickiness

APHIDS

Vegetal parts

Oil traces

Stickiness Waxes

WHITEFLIESPlant sugars

WHITEFLIES

Insect sugars

Origins of stickiness

Mature boll covered with honeydew

Origins of stickiness

Mature boll covered with honeydew

Origins of stickiness

Main sugars (in %) determined by HPLC in aphid, whitefly and aleurod honeydew, h t d G hi t

Mono- Polysaccharides

harvested on G. hirsutum

Sucrose Trehalulose MelezitoseAphis

Insect Mono-saccharides

Polysaccharides

Aphis gossypii 25 12 1 38

B i iBemisia tabaci 19 16 44 17

T i l dTrialeurodes abutilonea 44 33 3 0

Source Hendrix et al., 1992

Origins of stickiness

Th t i t t f ti ki i d t• The most important cause of stickiness is due to these entomological sugars.

• Honeydew has now become one of the maincontaminants present in cotton.p

• Sticky points remain in the cotton from the field up toh i i h h d ithe spinning processes where they cause productionand quality losses.

• The behavior of contaminated fibres duringprocessing is highly dependent upon the quantity andp g g y p p q ythe type of the main sugars present in fibres

Plan of presentation

I d iIntroduction

Stickiness: origins

Stickiness: measurementStickiness: measurement

Stickiness measurement

Simple PerkinsFehlingColor reactionKOTITI

Chemical methods

Complex

KOTITI

HPLCGCp GC

Physical techniques Infra-red

Mechanical Mini-card

ITMF Reference methodSCT

H2SD

FCT / FQT

ITMF Recommended method

Thermo-mechanical

FCT / FQT

Quickspin

Stickiness measurementSome measuring devices for stickiness evaluation

Credit: M. Watson

Stickiness measurementSome measuring devices for stickiness evaluation

Credit: M. Watson

Stickiness measurementSome measuring devices for stickiness evaluation

Credit: M. Watson

Stickiness measurementSome measuring devices for stickiness evaluation

Credit: M. Watson

Stickiness measurementSome measuring devices for stickiness evaluation

Credit: M. Watson

Stickiness measurementSome measuring devices for stickiness evaluation

Credit: M. Watson

Stickiness measurementSome measuring devices for stickiness evaluation

Credit: M. Watson

Bibliography on stickinessg yCauses, measurements and

consequencesconsequences

GOURLOT J PGOURLOT J.-P.ICCTM-ITMF, Stickiness WG

Bremen, March 2010

CIRAD UPR102Laboratoire de Technologie et de Caractérisation

des fibres naturelles

Introduction of the bibliography

• In order to allow everyone to learn more about this contamination, we decided to prepare this extract of the available literature. We retained around 214 references out of thousands of available references, focusing on the cause of stickiness, on the possible means of evaluation and/or measurement and on major consequences during fibre processing.

• The initial bibliography covers a period going from g p y p g gthe 1960’s to 2008.

Observation

Numberof documents on stickiness

60

70

Number of documents on stickiness

40

50

60

20

30

40

0

10

20

0

Observation

Numberof documents on stickiness

60

70

Number of documents on stickiness

40

50

60

20

30

40

0

10

20

0

PDF filePDF file

CIRAD UPR102Laboratoire de Technologie et de Caractérisation

des fibres naturelles

Thanks for attention and suggestionsThanks for attention … and suggestions

CIRAD UPR102Laboratoire de Technologie et de Caractérisation

des fibres naturelles

International Textile Manufacturers Federation (ITMF)

International Cotton CommitteeInternational Cotton Committee on Testing Methods (ICCTM)

Stickiness WG

Latest information

GOURLOT Jean-Paul Bremen March 2010

CIRAD UPR102

Bremen, March 2010

Laboratoire de Technologie et de Caractérisationdes fibres naturelles

Latest information ITMF - ICCTM 2010ITMF ICCTM 2010

SYDEL SA M t lli FSYDEL SA, Montpellier, France manufactures SCT and H2SDLintronics: no news since 2008 and beforeKOTITI: prepared an ISO standards thatKOTITI: prepared an ISO standards that currently comes to the National Standardization Bodies (AFNOR, DIN, …)No (public) patent this yearNo (public) patent this year

Latest information ITMF - ICCTM 2010ITMF ICCTM 2010

• SYDEL : Axes de développement de la nouvelle version (H2SDv2)– Coût Machine– Technologies Actuelles– Réduction du consommable– Des bases solides pour les développements futurs

• Différentiation du type de collage Mouche Blanche / Puceron (US patents)

• Evaluation du taux de collage par spectrométrie.– Un partenariat reconduit avec le CIRAD pour vérifier

le niveau de lecture et sa précision

Observation

Numberof documents on stickiness

60

70

Number of documents on stickiness

40

50

60

20

30

40

0

10

20

0

Latest information ITMF - ICCTM 2010ITMF ICCTM 2010

Cotton Contamination Survey 2009

30

Stickiness

27

21

24

perc

ent

15

18

151989 1991 1993 1995 1997 1999 2001 2003 2005 2007 2009

Thanks to M. Christian Schindler, ITMF

Thank you

forfor

your attentiony

CIRAD UPR102Laboratoire de Technologie et de Caractérisation

des fibres naturelles