SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20...
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Transcript of SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20...
![Page 1: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC.](https://reader036.fdocument.pub/reader036/viewer/2022062302/5706385d1a28abb8238fe4a6/html5/thumbnails/1.jpg)
SEIKO GROUP
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・ Sample: Azoxyanisole
・ DSC : DSC6200・ Sample :5 mg・ Scan Rate : 20 ゚
C/min
DSCDSC
![Page 3: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC.](https://reader036.fdocument.pub/reader036/viewer/2022062302/5706385d1a28abb8238fe4a6/html5/thumbnails/3.jpg)
Prensinhas e CadinhosPrensinhas e CadinhosSample Pan1-7 Sealed Type8-15 Open Type16-17 Hermetic Type
Panelinhas para alta pressão
DSCDSC
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Modelo DSC 7020 DSC 6100 DSC 6220 DSC 6300
Tipo de DSC Heat Flux DSC
Faixa de Temperatura -170 ~ 725°C -170 ~ 500°C -170 ~ 725°C Ambiente ~ 1500°C
Ruído Médio 0.1µW 0.1µW 0.2µW 10µW
Sensibilidade 0.2µW 0.2µW 0.4µW 20µW
Taxa de Aquecimento 0.01 ~ 100°C/min 0.01 ~ 20°C/min 0.01 ~ 100°C/min 0.01 ~ 100°C/min
Amostrador Automático Opcional Opcional Opcional Indisponível
Controlador de Gás de Purga Opcional Opcional Opcional Opcional
Capacidade Máxima: Open Pan 100µL 100µL 100µL 50µL
Capacidade Máxima: Hermetic Sealed 15µL 70µL 15µL
Capacidade Máxima: Sealed 15µL 15µL
Sistema Automático de Resfriamento com LN2
(Opcional)
-150 ~ 500°C -150 ~ 500°C -170 ~ 725°C Indisponível
Sistema Eletrônico de Resfriamento(Opcional)
-70 ~ 420°C C Type: -75 ~ 210°CD Type: -30 ~ 250°C
C Type: -75 ~ 470°CD Type: -30 ~ 380°C
Indisponível
Cooling Can (Opcional) -170 ~ 725°C -170 ~ 500°C -170 ~ 725°C Indisponível
DSCDSC
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DSCDSC
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DSC OVAL SENSORDSC OVAL SENSOR
Main Heat SinkMain Heat Sink
Oval Sensor PlateOval Sensor Plate
Sample PanSample PanReference Pan Reference Pan
Oval DSC DiagramOval DSC Diagram
Heater Heater
Oval Sensor PlateOval Sensor Plate
Main Heat SinkMain Heat Sink
Heat FilterHeat Filter
Lead WireLead Wire
Sub Heat Sink Sub Heat Sink
Oval DSC Cross SectionOval DSC Cross Section
・ ・ High Resolution (Quick responsibility)High Resolution (Quick responsibility) ・・ Low thermal resistance by 2nd dimension thermo flow Low thermal resistance by 2nd dimension thermo flow ・・ The shortest heat flow between sample and referenceThe shortest heat flow between sample and reference
・ ・ Protect the sensitivity down (by reducing noise lever)Protect the sensitivity down (by reducing noise lever)・ ・ Heat sink substrate used as sensor holder alsoHeat sink substrate used as sensor holder also・ ・ Filter stored inside sensor in order to cut the noise.Filter stored inside sensor in order to cut the noise.
DSCDSC
![Page 7: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC.](https://reader036.fdocument.pub/reader036/viewer/2022062302/5706385d1a28abb8238fe4a6/html5/thumbnails/7.jpg)
• Os DSCs da SII NanoTechnology – Seiko são os únicos DSCs com forno Elipsoidal.
• Melhor resolução, alta sensibilidade e excelente planicidade da linha base.
Exclusividade da SEIKO SII NanoTechnology
DSCDSC
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Full range Cooling system
Electronic Cooling System, Automatic LN2
cooling system
Robust Auto-sampler
DSCDSC
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Research & Development Application ー DTG(TG) and DSC peak separation. ( for reaction of different activation energies ) ー Data simulation of measurements that are difficult
such as extremely high ( ex. 106℃/min ) or extremely low heating rates ( ex. 10-3℃/min ) .
Reduced measurement time for Quality Control ー Measurement time → 1/2~1/10
Application of Highway TAApplication of Highway TATG/DTATG/DTA
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Measured Data
Separated Peak
Synthetic Peak
Peak SeparationPeak Separation
DSCDSC
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High and Low Heating Rate SimulationHigh and Low Heating Rate Simulation
DSCDSC
Temp Cel280.0260.0240.0220.0200.0180.0160.0140.0120.0
DSC
mW
0.00
-5.00
-10.00
-15.00
-20.00
Poliamida5ºC/min
10ºC/min
15ºC/min
20ºC/min25ºC/min