LAMPIRAN C1
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Transcript of LAMPIRAN C1
LAMPIRAN CHASIL ANTARA
C.1.Kalibrasi Termometer
Tabel C.1 Kalibasi termometer
TermometerPercobaanLiteratur
Tb (C)Td (C)Tb (C)Td (C)
Raksa 1195098,46
Raksa 2195098,46
Raksa 3195098,46
Raksa 4195098,46
Raksa 5195098,46
Gambar C.1 Kurva kalibrasi termometer
C.2.Kalibrasi Piknometer dan Penentuan Densitas MetanolC.2.1 Kalibrasi PiknometerTabel C.2 Kalibrasi piknometer
Massa piknometer kosong (kg)0,006681
Massa piknometer + aquadest (kg)0,008321
Massa aquadest (kg)0,00164
Densitas aquadest pada suhu 26,3 C (kg/m3)996,703
Volume piknometer (m3)1,645410-6
C.2.2 Penentuan Densitas MetanolTabel C.3 Penentuan densitas metanolMassa piknometer kosong (kg)0,006681
Massa piknometer + metanol (kg)0,00797
Massa metanol (kg)0,001289
Volume piknometer (m3)1,645410-6
Densitas metanol (kg/m3)783,384
C.3.Kalibrasi PompaTabel C.4 Kalibrasi pompa% Bukaan pompat(sekon)Volume (mL)Q (mL/s)Q(m3/s)
123Rata-rata
00000000
1030100100105101,673,3893,389x10-6
2030120125120121,674,0564,056 x10-6
30301701601651655,50,0000055
4030200210200203,336,7786,778 x10-6
503024025023024080,000008
60302802752702759,1679,167 x10-6
70302902952852909,6679,667 x10-6
803032031531031510,50,0000105
9030330330340333,3311,1111,111 x10-5
10030380370380376,6712,5561,256 x10-5
Gambar C.2 Kurva kalibrasi pompa
C.4Kalibrasi RefraktometerTabel C.5 Kalibrasi refraktometerIndeks BiasPercobaanLiteratur
AquadestBenzenaMetanolAquadestBenzenaMetanol
11,3350151,4958151,32851,3331,491,323
21,3350151,4958151,3291,3331,491,323
31,335021,4958151,32851,3331,491,323
Indeks Bias Rata-Rata1,335021,495821,328671,3331,491,323
Gambar C.3 Kurva kalibrasi refraktometer
C.5Penentuan Fraksi Mol Metanol Teknis Tabel C.6 Indeks bias metanol teknisZatIndeks BiasIndeks Bias Rata-rataIndeks Bias KoreksiFraksi Metanol Teknis
123
Metanol teknis1,3291,32951,32951,32931,324380,97
C.8Penentuan %Recovery Dari PercobaanTabel C.13 %Recovery percobaan distilasi selama 180 menitt(menit)Massa botol kosong (gram)Massa botol + distilat (gram)Massa distilat (gram)Jumlah (gram)Massa metanol umpan (gram)% Recovery
1067,60972,5694,96391,9591301,97630,105%
2067,60976,9879,378
3067,60973,6896,08
4067,60975,3587,749
5067,60978,2710,661
6067,60975,6128,003
7067,60989,92822,319
8067,60973,1185,509
9067,60977,98110,372
10067,60973,7216,112
11067,60983,04915,44
12067,60985,93618,327
13067,60984,73117,122
14067,609104,69237,083
15067,609127,46359,854
16067,609145,47677,867
17067,609122,74555,136
18067,60987,59619,987
Vacum000
C.9Penentuan HETPTabel C.14 HETP distilasi selama 180 menitJumlah tahap teoritis5
Tinggi kolom (cm)94
HETP18,8
C.10Penentuan Efisiensi TahapTabel C.15 Efisiensi tahap distilasi selama 180 menitJumlah tahap teoritis5
Jumlah tahap sebenarnya8
Efisiensi tahap57,143 %
C.11Penentuan Rasio RefluksTabel C.16 Rasio refluks distilasi selama 180 menitXD/Ropt +10,245
XD/Rmin +10,365
Ropt2,943673469
Rmin1,647123288
Faktor pengali (X)1,787160373
L51
D43
Ropt1,1860
Rasio refluks0,4029
C.12Penentuan Neraca Massa Distilasi KontinueTabel C.17 Neraca massa distilasi kontinueUmpan
Massa metanol teknis (gram)1019,939
Massa aquadest (gram)730,062
Massa umpan total (gram)1750,001
Keluaran
Total (gram)1009,959
Hilang (gram)740,0423
C.13Nilai Akhir Distilasi Kontinyu Refluks ParsialC.13.1BottomTabel C.18 Nilai akhir di bottomMassa bottom (gram)618
Indeks Bias11,338032
21,338031
31,338031
Rata-rata1,338031
Terkoreksi1,332975
X metanol0,083
LAMPIRAN EMSDS
LAMPIRAN:LAMPIRAN A : DATA LITERATURLAMPIRAN B : DATA PENGAMATANLAMPIRAN C : HASIL ANTARALAMPIRAN D : CONTOH PERHITUNGANLAMPIRAN E : MSDS